1). Bad guy death scenes so brutal you actually felt bad for the dude: In the last Rambo movie, it will be when Rambo just obliterated the driver's head at point blank with the mounted 50cal machine gun & what was, uh, "left" of him just fell off the jeep. Sure, he made have killed hundreds with the "landmine game" & threw a lot of babies into fires, but for all we know, that dude was just following orders & had no choice. On the other hand, the leader dude got what he deserved.
2). Poisoning: In Casino Royale, when Le Chiffre has his hot girlfriend poison Bond's drink & Bond just barely survives.
3). Most impressive shape-shifting technology: Instead of going with robots that begin with the letter 'T', I'll go with the vechicles from the M.A.S.K. cartoon. A car that can fly by using its doors as wings(?), a helicopter that can turn into a plane, or a speedboat that can come out of a jeep. (OK, so maybe the jeep example wasn't so impressive.)